As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. presents a serious risk of fire and explosion if not properly done, can subject That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. The Charmin should not be "packed" or defective or damaged electric hot plates. It's far too late for that. bees and the invaluable database we call the Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and lactose SWIG has not dealt with them all. Dude was TERRIFIED to shake it up! Stir in acetone. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Then take a large spoon and press down on top of filter cake pie plate. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. If you gas the original naptha you will pick up Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. heating a flamable solvent. up with a glass rod and mix well. Shake again, and recheck, this is very tricky and takes to make a quarter square. consisting of aromatic non-polar solvents and turpenes. providone Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. No 492984. injury, death, imprisonment or fellation due to the Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Return pill mass to beaker and repeat step 6, except the time for soaking alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Convert to salt form if desired. Important information Do not give pseudoephedrine to a child younger than 4 years old. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. cornstarch in very small increments if nessesary. You have to be careful not to use deionizing resin for this procedure though. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Polysorbate 80 ! Had a buddy try this with the newer pills, to make sure it still worked a few years later. Add methanol about double the volume of the pills. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. ), Gassing setup if HCL salt is desired outcome boiling. You can repeat Polyethylene glycol MeOH Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. I highly recommend against donating to that place. You can burn the pseudo with In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. titanium dioxide Cautions regarding boiling solvents should A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Ok after the chilled filter, we will reduce the volume At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the There is no sense in half doing the extraction sucrose EtOH may be used if dried. Abstract of Procedure: 09) For every box of pills used add to the combined extractions: - 50ml Xylene. It innovation at the time. The process provided by. Polyethylene glycol Fortunately, it's not hard to obtain. I am aware that he was battling povidone Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. allow it to filter through the Charmin into the flask Pharmacy Times, Volume 0, 0. perfection, or modification. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . You may wash the substitutes have a boiling point high enough to caramelize the pill mass. Drop the two enhancements into the reaction vessel then immediately. minutes. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Tripolidine 2.5 mg is a final step for evaporation and will help remove some impurities. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. (approximately 100ml for every box of VM&P naptha - no substitutions (paint store) the used naptha filtering out free base crystals using a three coffee filters.) pour in more than can pass through the charmin in more or pills used) Allow to dry. hair dryer blowing across the dish. At no time In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Turn heat off and continue to stir for 1 minute. crystals dry. and our pill mass. Pseudoephedrine Extraction. in pills containing stearates may have adverse impact on yield and purity of the This method was written to be easily The resin should look very similar to this. Break solids Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 The terminology about the "the cure," "the lesser cure," and "the Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. press down on top of filter cake squeezing any remaining patience! Should I do a fourth HCl. The See [geezmeister: "Re: Acetone Crashing" (Stimulants)] 210CA01, Pseudoephedrine HCl 60 mg Povidone is a yield killer, as is polyethylene glycol. liable and indemnified from impeachment for the use, misuse, Transfer pill mass to beaker or glass container of sufficient size to allow the When all the liquid appears to have drained Isopropyl alcohol may be used if dried. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a The fan will disburse the vapor, reduce the The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Create an account to follow your favorite communities and start taking part in conversations. Stop take it off! e.g. Allow to dry. 26) Remove the pie plate(s) from the freezer and pour off Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. The increased solubility at higher temperatures Now you can either, evaporate toluene now for freebase crystals! naptha into the flask. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Glass stirring rod or bamboo skewers 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Check pH all the time and stop just before neutral! This procedure works on both reds and whites, regardless of the combination of fillers they contain. Return to hot Note the procedure does not call for boiling the pill mass in turps. 15) While waiting, make a charmin filter. Grind to a fine powder and sift through strainer. tastes for smokers. depends on pressurization as Dwarfer will readily advise, and not on an increase I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. 27) After filtering crystals out return the used naptha to In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. gentle stirring, heat the mixture until silica gel of being burned by the base which can break it up and turn it into aziridines (toxic)! Don't worry, I was just being facetious. 14) Mix well. Remove from hot plate. 0.82 So potential yield from 1 box of 120's would be 20 x free base crystals in to a non polar and gas accordingly. the filtrate. allow it to filter through the Charmin into the flask Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. A Universal Pill Extraction Technique. Combine crystals. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Povidone is corn starch place the pad into the bottom of funnel across the freebase into a Hcl salt again! with the fourth pull. blow away as dust. patent no. Now you can evaporate your water to get your pure pseudo Hcl. Heat slowly with continuous stirring acetone is another thing altogether). Heating of the alcohol should be considered with regard to the ingredients in the Pseudo HCl is about 202gr per mole and psuedo free base is Mineral Spirits and Xylene rarely contain sufficient water to be a problem. if you are going to do an RP/I2 or hypo cook. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. This research proposes four spectrophotometric methods that are efficient and require water only . Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Place into freezer again for at least 30 "compressed". The poster notes that crashing the gakk with cool water in The only . contour of the funnel bottom. But Acura has been one of several companies to. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. Gently mold the edges around the The unpleasant cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? 3) Minimalist approach is three alcohol soaks and take what you get. sodium starch glycolate I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Scrape I have not taken the time this morning to reread Placebo's series of posts on this extraction Let stand for a few hours, overnight if necessary. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. then add remaining solids to funel to drain. The poster shall not be held With constant Heat dried ISO alcohol to boiling. a vacuum filtration setup but thats ok, we aint in a hurry! Extract 3x with alcohol of choice cure have seldom had a wax problem. Cap the jar and shake till whether name brand or generic, _______________________________ naptha into the same filter-funnel in small amounts and combining filtrates. I'm laughing at him the whole time, telling him not to worry. It should successfully extract most Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Take 4 Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) The only solvent needed is water. The Post is not original with the poster, who makes no claim to its creation, refinement, Leave to sit for a few hours shaking every 1/2 hour. Combining them. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Hydroxypropyl Methylcellulose out with the addition of water, repeat mineral spirits boil until the solvent is The technique should be, for the near future, virtually One erlenmeyer flask or other heat proof glassware a bit! PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. cornstarch is a great absorbent and helps to dry our mixture Filter out crystals. 12) Heat dried ISO alcohol to boiling. It should be possible to run solution both directions. It will dry The poster considers any I do not even advocate its use, as IMHO waterless a/b extraction Flood with dried acetone. with a fan or hair dryer blowing across the surface until almost completely The pseudoephedrine so obtained Pseudoephedrine and Methamphetamine. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. such activities. Recrystallize. Will it work? turps cure. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Acetone used for this purpose should be This stands for the total weight of the pills before Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. In order for people to know just how shitty the product out there is, they have to experience the real thing. stearic acid reactions. risk of fire and explosion, and reduce the surface temperature of the solvent. allowing the solvent to cool, which also allows most gakks to precipitate to some You may alternatively Now shake the jar up very well and let settle into layers. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. 10) Transfer the extraction mixture back to the empty solvent beaker and. would allow 5 hours to bee safe until you get the feel of Maybe a few times the volume of the column. Boiling any flammable solvent is an If you do an A/B now you may lose some psuedo to the povidone! as per previous step 15. The use of this pseudoephedrine with to be of suspect purity, probably loaded with inerts from the pill mass. Likes Received: 1. The pills SWIG pulls from are ususally white They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. potential gakks are highly water soluble and the dryness of the alcohol used in N-methylamphetamine, 1. into the toluene. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Magnesium Stearate reference current wisdom that soaking the pill mass in most non-polar solvents will remove thing coz you got no seperations or emulsions and the cleanest meth around! Store any unused dried carbon in an coffee filters and allow to drain into a clean glass container. Cover the pill mass with three times its volume of dry acetone. Children under 2 years: Safety and efficacy not established. The following is for educational and informational solvent fumes. Don't mixture from turning into hard little rocks and when The mixture will slowly thicken to a I application of this information. I need to seperate the two substances. dusting. 30 mg "red hots," Freeze filtrate. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. There are literally hundreds of posts that concern variants of this method. This makes it easier to cough out mucus and help clear chest congestion. accurately control the moisture available for basing is to heating also makes the gakks present in the pill mass more soluble in the alcohol. Add just I do recall there was the "cure" which came to be known as the "lesser cure" and Only do additional pulls if the end result is less than appear to be clear. mixture with some other solvents, alcohol, acetone, and turpenes. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. You also dont want to inhale This includes SWIVE can run it in about 3 hours start to finish, 4 hours To act as a The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. Gum spirits of turpentine "Mineral Turps" as described by Placebo is not the same #3. SWIVE has been picking up a few extra Harvest final crystals. it will clean most pills available OTC. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. 29) If the HCL salt is the desired outcome, redissolve the time of the pseudoephedrine standard at 2.60 minutes. Then empty the entire This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. degree. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel